C₁₃H₁₉FN₂

Base Information

Chemical Name:C₁₃H₁₉FN₂
CAS No.:1269602-89-2
Molecular Formula:C₁₃H₁₉FN₂
Molecular Weight:222.306
Hs Code.:

C<sub>13</sub>H<sub>19</sub>FN<sub>2</sub>

Synonyms:C₁₃H₁₉FN₂

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Chemical Property of C₁₃H₁₉FN₂

Chemical Property:

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Technology Process of C₁₃H₁₉FN₂

There total 5 articles about C₁₃H₁₉FN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1384448-06-9
C₂₀H₂₅FN₂O₂S

: 1269602-89-2
C₁₃H₁₉FN₂

Guidance literature:: C₂₀H₂₅FN₂O₂S; With hydrogen bromide; acetic acid; 4-hydroxy-benzoic acid; at 20 ℃; for 48h; Inert atmosphere;

With water; for 2h;

Reference yield:

: 445-27-2
2'-Fluoroacetophenone

: 1269602-89-2
C₁₃H₁₉FN₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 1 h / -70 °C / Inert atmosphere

2.1: trifluoroacetic acid; sodium azide / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3.1: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / 20 h / 125 °C / Inert atmosphere

5.1: 4-hydroxy-benzoic acid; hydrogen bromide; acetic acid / 48 h / 20 °C / Inert atmosphere

5.2: 2 h

With sodium azide; hydrogen bromide; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; 4-hydroxy-benzoic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 320-12-7
2-(2'-fluorophenyl)propan-2-ol

: 1269602-89-2
C₁₃H₁₉FN₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid; sodium azide / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / 20 h / 125 °C / Inert atmosphere

4.1: 4-hydroxy-benzoic acid; hydrogen bromide; acetic acid / 48 h / 20 °C / Inert atmosphere

4.2: 2 h

With sodium azide; hydrogen bromide; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; 4-hydroxy-benzoic acid; palladium 10% on activated carbon; In methanol; dichloromethane;