2-Phenyl-[1,3]dioxane-5,5-dicarboxylic acid bis-[((S)-1-hydroxymethyl-2,2-dimethyl-propyl)-amide]

Base Information

Chemical Name:2-Phenyl-[1,3]dioxane-5,5-dicarboxylic acid bis-[((S)-1-hydroxymethyl-2,2-dimethyl-propyl)-amide]
CAS No.:853065-12-0
Molecular Formula:C₂₄H₃₈N₂O₆
Molecular Weight:450.576
Hs Code.:

Synonyms:2-Phenyl-[1,3]dioxane-5,5-dicarboxylic acid bis-[((S)-1-hydroxymethyl-2,2-dimethyl-propyl)-amide]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Phenyl-[1,3]dioxane-5,5-dicarboxylic acid bis-[((S)-1-hydroxymethyl-2,2-dimethyl-propyl)-amide]

Chemical Property:

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Technology Process of 2-Phenyl-[1,3]dioxane-5,5-dicarboxylic acid bis-[((S)-1-hydroxymethyl-2,2-dimethyl-propyl)-amide]

There total 3 articles about 2-Phenyl-[1,3]dioxane-5,5-dicarboxylic acid bis-[((S)-1-hydroxymethyl-2,2-dimethyl-propyl)-amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: Lithium; (S)-2-amino-3,3-dimethyl-butan-1-olate

: 71348-41-9
diethyl 6-phenyl-[1,5]-dioxane-3,3-dicarboxylic acid diester

: 853065-12-0
2-Phenyl-[1,3]dioxane-5,5-dicarboxylic acid bis-[((S)-1-hydroxymethyl-2,2-dimethyl-propyl)-amide]

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1016/j.tetasy.2005.02.026

Reference yield:

: 20605-01-0
diethyl bis(hydroxymethyl)malonate

: 853065-12-0
2-Phenyl-[1,3]dioxane-5,5-dicarboxylic acid bis-[((S)-1-hydroxymethyl-2,2-dimethyl-propyl)-amide]

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / p-TsOH / toluene / Heating

2: 45 percent / tetrahydrofuran / 16 h / 20 °C

With toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1016/j.tetasy.2005.02.026

Reference yield:

: 100-52-7
benzaldehyde

: 853065-12-0
2-Phenyl-[1,3]dioxane-5,5-dicarboxylic acid bis-[((S)-1-hydroxymethyl-2,2-dimethyl-propyl)-amide]

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / p-TsOH / toluene / Heating

2: 45 percent / tetrahydrofuran / 16 h / 20 °C

With toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1016/j.tetasy.2005.02.026