5-(3-aminophenylthio)-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine

Base Information

Chemical Name:5-(3-aminophenylthio)-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine
CAS No.:1268273-68-2
Molecular Formula:C₂₈H₃₀N₄O₄S
Molecular Weight:518.637
Hs Code.:

Synonyms:5-(3-aminophenylthio)-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine

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Chemical Property of 5-(3-aminophenylthio)-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine

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Technology Process of 5-(3-aminophenylthio)-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine

There total 4 articles about 5-(3-aminophenylthio)-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 22948-02-3
3-aminothiophenol

: 1268273-16-0
5-iodo-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine

: 1268273-68-2
5-(3-aminophenylthio)-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine

Guidance literature:: With potassium carbonate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; In dimethyl sulfoxide; at 125 ℃; for 20h; Inert atmosphere;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1268273-68-2
5-(3-aminophenylthio)-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

1.2: 20 °C

2.1: N-iodo-succinimide / acetonitrile / 1 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline / dimethyl sulfoxide / 20 h / 125 °C / Inert atmosphere

With N-iodo-succinimide; sodium hydride; potassium carbonate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 36315-01-2,256642-28-1
4,6-dimethoxy-2-aminopyrimidine

: 1268273-68-2
5-(3-aminophenylthio)-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

1.2: 20 °C

2.1: N-iodo-succinimide / acetonitrile / 1 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline / dimethyl sulfoxide / 20 h / 125 °C / Inert atmosphere

With N-iodo-succinimide; sodium hydride; potassium carbonate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;