Technology Process of C39H48N4O3S
There total 7 articles about C39H48N4O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 82 percent / lithium aluminium hydride / tetrahydrofuran / 3 h / Heating
2: 62 percent / NBS; PPh3 / CH2Cl2 / 20 °C
3: 81 percent / K2CO3 / dimethylformamide / 60 °C
4: 93 percent / PBu3; diisopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C
5: 97 percent / 2-mercaptoethanol; Cs2CO3 / dimethylformamide / 2 h
With
N-Bromosuccinimide; lithium aluminium tetrahydride; tributylphosphine; di-isopropyl azodicarboxylate; potassium carbonate; caesium carbonate; triphenylphosphine; 2-hydroxyethanethiol;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
4: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2007.03.024
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: NaOH
1.2: 50 percent / aq. HCl
2.1: 81 percent / K2CO3 / dimethylformamide / 60 °C
3.1: 93 percent / PBu3; diisopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C
4.1: 97 percent / 2-mercaptoethanol; Cs2CO3 / dimethylformamide / 2 h
With
sodium hydroxide; tributylphosphine; di-isopropyl azodicarboxylate; potassium carbonate; caesium carbonate; 2-hydroxyethanethiol;
In
tetrahydrofuran; N,N-dimethyl-formamide;
3.1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2007.03.024
