butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside
CAS No.:326594-72-3
Molecular Formula:C₃₁H₃₈O₆
Molecular Weight:506.639
Hs Code.:

Synonyms:butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

There total 4 articles about butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-butoxy-6-trityloxymethyl-tetrahydro-pyran

: 326594-72-3
butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With pyridine hydrochloride; In ethanol; for 2h; Heating;
DOI:10.1080/07328300008544141

Reference yield:

: 100-39-0
benzyl bromide

: 326594-72-3
butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dimethylformamide; various solvent(s) / 24 h / 0 - 20 °C

2: 1.31 g / pyridinium chloride / ethanol / 2 h / Heating

With pyridine hydrochloride; sodium hydride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/07328300008544141

Reference yield:

: 5391-18-4,25320-93-8,39824-09-4,95531-15-0,143289-25-2,146453-36-3,148347-27-7,41444-57-9
n-butyl β-D-glucopyranoside

: 326594-72-3
butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; 4-(dimethylamino)pyridine / dimethylformamide / 40 h / 35 °C

2: sodium hydride / dimethylformamide; various solvent(s) / 24 h / 0 - 20 °C

3: 1.31 g / pyridinium chloride / ethanol / 2 h / Heating

With dmap; pyridine hydrochloride; sodium hydride; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/07328300008544141