bis-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinate

Base Information

• Chemical Name: bis-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinate
• CAS No.: 326594-73-4
• Molecular Formula: C₆₆H₇₈O₁₄
• Molecular Weight: 1095.34
• Mol file: 326594-73-4.mol

Synonyms:bis-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinate

Chemical Property of bis-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinate

There total 5 articles about bis-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

succinoyl dichloride (543-20-4) + butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside (326594-72-3) → 4-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinic acid + bis-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinate (326594-73-4)

Guidance literature:

With triethylamine; In toluene; at 20 ℃;

DOI:10.1080/07328300008544141

Reference yield:

benzyl bromide (100-39-0) → bis-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinate (326594-73-4)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydride / dimethylformamide; various solvent(s) / 24 h / 0 - 20 °C

2: 1.31 g / pyridinium chloride / ethanol / 2 h / Heating

3: 50 percent / triethylamine / toluene / 20 °C

With pyridine hydrochloride; sodium hydride; triethylamine; In ethanol; N,N-dimethyl-formamide; toluene;

DOI:10.1080/07328300008544141

Reference yield:

n-butyl β-D-glucopyranoside (5391-18-4,25320-93-8,39824-09-4,95531-15-0,143289-25-2,146453-36-3,148347-27-7,41444-57-9) → bis-(butyl 2,3,4-tri-O-benzyl-β-D-glucopyranosid-6-yl) succinate (326594-73-4)

Guidance literature:

Multi-step reaction with 4 steps

1: triethylamine; 4-(dimethylamino)pyridine / dimethylformamide / 40 h / 35 °C

2: sodium hydride / dimethylformamide; various solvent(s) / 24 h / 0 - 20 °C

3: 1.31 g / pyridinium chloride / ethanol / 2 h / Heating

4: 50 percent / triethylamine / toluene / 20 °C

With dmap; pyridine hydrochloride; sodium hydride; triethylamine; In ethanol; N,N-dimethyl-formamide; toluene;

DOI:10.1080/07328300008544141

upstream raw materials:

succinoyl dichloride

butyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

benzyl bromide

n-butyl β-D-glucopyranoside