N-(diphenylmethyl)-2-iodo-4-nitroaniline

Base Information

• Chemical Name: N-(diphenylmethyl)-2-iodo-4-nitroaniline
• CAS No.: 540526-55-4
• Molecular Formula: C₁₉H₁₅IN₂O₂
• Molecular Weight: 430.245
• Mol file: 540526-55-4.mol

Synonyms:N-(diphenylmethyl)-2-iodo-4-nitroaniline

Chemical Property of N-(diphenylmethyl)-2-iodo-4-nitroaniline

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-(diphenylmethyl)-2-iodo-4-nitroaniline

There total 1 articles about N-(diphenylmethyl)-2-iodo-4-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2-iodo-4-nitrophenylamine (6293-83-0) + Bromodiphenylmethane (776-74-9) → N-(diphenylmethyl)-2-iodo-4-nitroaniline (540526-55-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; at 50 ℃; for 20h;

DOI:10.1021/jm061131z

Reference yield:

N-(diphenylmethyl)-2-iodo-4-nitroaniline (540526-55-4) → C40H37N3O7S (934285-72-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 61 percent / aq. NaHCO₃ / CH₂Cl₂

With sodium hydrogencarbonate; In dichloromethane; 2: Schotten-Baumann reaction;

DOI:10.1021/jm061131z

Reference yield:

N-(diphenylmethyl)-2-iodo-4-nitroaniline (540526-55-4) → C40H37N3O7S (1027233-56-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaHCO₃ / CH₂Cl₂

With sodium hydrogencarbonate; In dichloromethane; 2: Schotten-Baumann reaction;

DOI:10.1021/jm061131z

upstream raw materials:

2-iodo-4-nitrophenylamine

Bromodiphenylmethane

Downstream raw materials:

C₄₀H₃₇N₃O₇S

C₄₀H₃₇N₃O₇S

Refernces