(S)-2-hydroxy-2-methyl-4-(2-phenylmethoxy)butyl methanesulphonate

Base Information

Chemical Name:(S)-2-hydroxy-2-methyl-4-(2-phenylmethoxy)butyl methanesulphonate
CAS No.:131700-30-6
Molecular Formula:C₁₃H₂₀O₅S
Molecular Weight:288.365
Hs Code.:

Synonyms:(S)-2-hydroxy-2-methyl-4-(2-phenylmethoxy)butyl methanesulphonate

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Chemical Property of (S)-2-hydroxy-2-methyl-4-(2-phenylmethoxy)butyl methanesulphonate

Chemical Property:

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Technology Process of (S)-2-hydroxy-2-methyl-4-(2-phenylmethoxy)butyl methanesulphonate

There total 7 articles about (S)-2-hydroxy-2-methyl-4-(2-phenylmethoxy)butyl methanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 131700-29-3
(S)-2-methyl-4-(2-phenylmethoxy)butane-1,2-diol

: 124-63-0
methanesulfonyl chloride

: 131700-30-6
(S)-2-hydroxy-2-methyl-4-(2-phenylmethoxy)butyl methanesulphonate

Guidance literature:: With triethylamine; In dichloromethane; at -10 ℃; for 0.166667h;
DOI:10.1016/S0957-4166(00)86350-8

Reference yield:

: 64018-43-5
2-[(4S)-2,2,4-trimethyl-1,3-dioxolan-4-yl]ethanol

: 131700-30-6
(S)-2-hydroxy-2-methyl-4-(2-phenylmethoxy)butyl methanesulphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran

1.2: tetrabutylammonium iodide / tetrahydrofuran

2.1: aq. H₂SO₄ / tetrahydrofuran / 40 °C

3.1: Et₃N / CH₂Cl₂ / -10 °C

With sulfuric acid; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; 1.1: deprotonation / 1.2: benzylation / 2.1: Hydrolysis / 3.1: Esterification;
DOI:10.1071/CH99091

Reference yield:

: 6236-09-5,2306-22-1
(S)-citramalic acid

: 131700-30-6
(S)-2-hydroxy-2-methyl-4-(2-phenylmethoxy)butyl methanesulphonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: CH₂Cl₂; ethanol

2.1: LiAlH₄ / tetrahydrofuran / Heating

3.1: p-toluenesulfonic acid / 20 °C

4.1: NaH / tetrahydrofuran

4.2: tetrabutylammonium iodide / tetrahydrofuran

5.1: aq. H₂SO₄ / tetrahydrofuran / 40 °C

6.1: Et₃N / CH₂Cl₂ / -10 °C

With lithium aluminium tetrahydride; sulfuric acid; sodium hydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; 1.1: Esterification / 2.1: Reduction / 3.1: cyclocondensation / 4.1: deprotonation / 4.2: benzylation / 5.1: Hydrolysis / 6.1: Esterification;
DOI:10.1071/CH99091