methyl 5-O-benzoyl-3-deoxy-3-fluoro-2-O-(imidazol-2-ylsulfonyl)-α-D-ribofuranoside

Base Information

Chemical Name:methyl 5-O-benzoyl-3-deoxy-3-fluoro-2-O-(imidazol-2-ylsulfonyl)-α-D-ribofuranoside
CAS No.:1203460-74-5
Molecular Formula:C₁₆H₁₇FN₂O₇S
Molecular Weight:400.385
Hs Code.:

Synonyms:methyl 5-O-benzoyl-3-deoxy-3-fluoro-2-O-(imidazol-2-ylsulfonyl)-α-D-ribofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 5-O-benzoyl-3-deoxy-3-fluoro-2-O-(imidazol-2-ylsulfonyl)-α-D-ribofuranoside

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Technology Process of methyl 5-O-benzoyl-3-deoxy-3-fluoro-2-O-(imidazol-2-ylsulfonyl)-α-D-ribofuranoside

There total 2 articles about methyl 5-O-benzoyl-3-deoxy-3-fluoro-2-O-(imidazol-2-ylsulfonyl)-α-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 288-32-4
1H-imidazole

: 237410-13-8
((2R,3S,4S,5S)-3-fluoro-4-hydroxy-5-methoxytetrahydrofuran-2-yl)methyl benzoate

: 1203460-74-5
methyl 5-O-benzoyl-3-deoxy-3-fluoro-2-O-(imidazol-2-ylsulfonyl)-α-D-ribofuranoside

Guidance literature:: ((2R,3S,4S,5S)-3-fluoro-4-hydroxy-5-methoxytetrahydrofuran-2-yl)methyl benzoate; With sulfuryl dichloride; In dichloromethane; N,N-dimethyl-formamide; at -40 - 20 ℃;

1H-imidazole; In dichloromethane; N,N-dimethyl-formamide; at 18 ℃;
DOI:10.1080/15257770903053979

Reference yield:

: C₉H₁₃FN₂O₆S

: 98-88-4
benzoyl chloride

: 1203460-74-5
methyl 5-O-benzoyl-3-deoxy-3-fluoro-2-O-(imidazol-2-ylsulfonyl)-α-D-ribofuranoside

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1080/15257770903053979

Reference yield: 49.0%

: 1203460-74-5
methyl 5-O-benzoyl-3-deoxy-3-fluoro-2-O-(imidazol-2-ylsulfonyl)-α-D-ribofuranoside

: 237410-14-9
methyl 5-O-benzoyl-2,3-dideoxy-2,3-difluoro-α-D-arabinofuranoside

Guidance literature:: With potassium hydrogen bifluoride; hydrogen fluoride; In water; 2.3-butanediol; at 160 ℃; for 0.833333h; Inert atmosphere;
DOI:10.1080/15257770903053979