4,5-dichloro-1,3-bis(4-methoxybenzyl)imidazolium bromide

Base Information

Chemical Name:4,5-dichloro-1,3-bis(4-methoxybenzyl)imidazolium bromide
CAS No.:1234568-59-2
Molecular Formula:Br*C₁₉H₁₉Cl₂N₂O₂
Molecular Weight:458.182
Hs Code.:

Synonyms:4,5-dichloro-1,3-bis(4-methoxybenzyl)imidazolium bromide

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Chemical Property of 4,5-dichloro-1,3-bis(4-methoxybenzyl)imidazolium bromide

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Technology Process of 4,5-dichloro-1,3-bis(4-methoxybenzyl)imidazolium bromide

There total 1 articles about 4,5-dichloro-1,3-bis(4-methoxybenzyl)imidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.8%

: 2746-25-0
p-Methoxybenzyl bromide

: 15965-30-7
4,5-dichloroimidazole

: 1234568-59-2
4,5-dichloro-1,3-bis(4-methoxybenzyl)imidazolium bromide

Guidance literature:: 4,5-dichloroimidazole; With potassium carbonate; In acetonitrile; for 0.25h;

p-Methoxybenzyl bromide; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1002/ejic.200900889

Reference yield: 72.7%

: 1234568-59-2
4,5-dichloro-1,3-bis(4-methoxybenzyl)imidazolium bromide

: 563-63-3
silver(I) acetate

: (4,5-dichloro-1,3-bis(4-methoxybenzyl)imidazol-2-ylidene)silver(I) acetate

Guidance literature:: In dichloromethane; byproducts: AgBr; ligand dissolved in CH2Cl2, treated with 2 equiv. of AgOAc, stirred in the dark at room temp. for 2 d; AgBr filtered off, evapd.(vac.), washed (hexane), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200900889