2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxymethyl]benzofuran

Base Information

Chemical Name:2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxymethyl]benzofuran
CAS No.:854371-75-8
Molecular Formula:C₂₁H₂₃BO₄
Molecular Weight:350.222
Hs Code.:

Synonyms:2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxymethyl]benzofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxymethyl]benzofuran

Chemical Property:

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Technology Process of 2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxymethyl]benzofuran

There total 1 articles about 2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxymethyl]benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 41014-27-1
2-bromomethylbenzofuran

: 269409-70-3
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

: 854371-75-8
2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxymethyl]benzofuran

Guidance literature:: With potassium carbonate; In acetonitrile; at 70 ℃; for 16h;
DOI:10.1016/j.bmc.2005.07.076

Reference yield: 33.0%

: 854371-75-8
2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxymethyl]benzofuran

: 779341-90-1
(R)-2-(4-bromobenzenesulfonylamino)-3-methylbutyric acid tert-butyl ester

: 854371-76-9
D-2-[4'-(benzofuran-2-ylmethoxy)biphenyl-4-sulfonylamino]-3-methylbutyric acid tert-butyl ester

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 90 ℃; for 8h;
DOI:10.1016/j.bmc.2005.07.076

Reference yield:

: 854371-75-8
2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxymethyl]benzofuran

: D-2-[4'-(benzofuran-2-ylmethoxy)-biphenyl-4-sulfonylamino]-3-methyl-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / K₂CO₃ / Pd(PPh₃)4 / 1,2-dimethoxy-ethane; H₂O / 8 h / 90 °C

2: 25 percent / cerium(III) chloride heptahydrate; KI / acetonitrile / 16 h / Heating

With cerium(III) chloride; potassium carbonate; potassium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; acetonitrile; 1: Suzuki coupling;
DOI:10.1016/j.bmc.2005.07.076