C₁₇H₁₈BrNO

Base Information

Chemical Name:C₁₇H₁₈BrNO
CAS No.:1338797-52-6
Molecular Formula:C₁₇H₁₈BrNO
Molecular Weight:332.24
Hs Code.:

Synonyms:C₁₇H₁₈BrNO

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Chemical Property of C₁₇H₁₈BrNO

Chemical Property:

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Technology Process of C₁₇H₁₈BrNO

There total 10 articles about C₁₇H₁₈BrNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₀BrNO₂Si

: 1338797-52-6
C₁₇H₁₈BrNO

Guidance literature:: With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; In methanol; at -30 - 25 ℃; for 2h;
DOI:10.3390/molecules23102607

Reference yield:

: 1338796-89-6
1-bromo-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-one

: 1338797-53-7
C₁₇H₁₈BrNO

: 1338797-52-6
C₁₇H₁₈BrNO

Guidance literature:: 1-bromo-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-one; With trimethylsilyl trifluoromethanesulfonate; triethylamine; In toluene; at 80 ℃; for 4h; Inert atmosphere;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 3h; Further stages; Inert atmosphere;
DOI:10.1016/j.bmc.2011.06.089

Reference yield:

: C₂₃H₂₉BrO₂Si

: 1338797-52-6
C₁₇H₁₈BrNO

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine hydrochloride / pyridine / 5 h / 25 °C

1.2: 2 h / 25 °C

2.1: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / methanol / 2 h / -30 - 25 °C

With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; hydroxylamine hydrochloride; In pyridine; methanol;
DOI:10.3390/molecules23102607