C₆₂H₆₇Cl₃N₂O₁₆

Base Information

Chemical Name:C₆₂H₆₇Cl₃N₂O₁₆
CAS No.:1415996-38-1
Molecular Formula:C₆₂H₆₇Cl₃N₂O₁₆
Molecular Weight:1202.58
Hs Code.:

C<sub>62</sub>H<sub>67</sub>Cl<sub>3</sub>N<sub>2</sub>O<sub>16</sub>

Synonyms:C₆₂H₆₇Cl₃N₂O₁₆

Suppliers and Price of C₆₂H₆₇Cl₃N₂O₁₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₂H₆₇Cl₃N₂O₁₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₂H₆₇Cl₃N₂O₁₆

There total 15 articles about C₆₂H₆₇Cl₃N₂O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: C₅₉H₆₆N₂O₁₄

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 1415996-38-1
C₆₂H₆₇Cl₃N₂O₁₆

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water; at 0 ℃; for 0.166667h;
DOI:10.1039/c2ob26928g

Reference yield:

: 460082-41-1
phenyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 1415996-38-1
C₆₂H₆₇Cl₃N₂O₁₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 5 h / -10 °C / Molecular sieve; Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane; methanol / 0.5 h / 0 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 6 h / 0 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

5.1: 1,1'-sulfinylbisbenzene; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine / dichloromethane / -60 - -40 °C / Molecular sieve; Inert atmosphere

5.2: -60 - 20 °C / Inert atmosphere

6.1: thiourea; 2,6-dimethylpyridine / N,N-dimethyl-formamide / 12 h / 50 °C

7.1: 1.3-propanedithiol; triethylamine / tetrahydrofuran; methanol / 48 h / 20 °C

8.1: sodium hydrogencarbonate / water; tetrahydrofuran / 0.17 h / 0 °C

With 2,6-dimethylpyridine; 1.3-propanedithiol; N-iodo-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; [bis(acetoxy)iodo]benzene; 1,1'-sulfinylbisbenzene; sodium hydrogencarbonate; potassium carbonate; triethylamine; thiourea; trifluoroacetic acid; 2,4,6-tri-tert-butylpyrimidine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26928g

Reference yield:

: 183875-35-6
phenyl 3,4,6-tri-O-acetyl-2-deoxy-2-azido-1-thiol-α-D-glucopyranoside

: 1415996-38-1
C₆₂H₆₇Cl₃N₂O₁₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium methylate / methanol / 5 h / 20 °C

2.1: trimethyl orthoformate; camphor-10-sulfonic acid / N,N-dimethyl-formamide / 36 h / 70 °C

3.1: sodium hydride / tetrahydrofuran / 0 - 20 °C

4.1: trimethylamine-borane; aluminum (III) chloride / tetrahydrofuran / 24 h / 20 °C / Molecular sieve

5.1: pyridine / dichloromethane / 0 - 20 °C

6.1: N-Bromosuccinimide; water / acetone / 6 h / 0 °C

7.1: 1,1'-sulfinylbisbenzene; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine / dichloromethane / -60 - -40 °C / Molecular sieve; Inert atmosphere

7.2: -60 - 20 °C / Inert atmosphere

8.1: thiourea; 2,6-dimethylpyridine / N,N-dimethyl-formamide / 12 h / 50 °C

9.1: 1.3-propanedithiol; triethylamine / tetrahydrofuran; methanol / 48 h / 20 °C

10.1: sodium hydrogencarbonate / water; tetrahydrofuran / 0.17 h / 0 °C

With pyridine; 2,6-dimethylpyridine; 1.3-propanedithiol; aluminum (III) chloride; N-Bromosuccinimide; trifluoromethylsulfonic anhydride; trimethylamine-borane; 1,1'-sulfinylbisbenzene; camphor-10-sulfonic acid; water; sodium methylate; sodium hydride; sodium hydrogencarbonate; triethylamine; thiourea; 2,4,6-tri-tert-butylpyrimidine; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c2ob26928g