[2-(3,4-Dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-8-ylidene)-amine

Base Information

Chemical Name:[2-(3,4-Dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-8-ylidene)-amine
CAS No.:129881-26-1
Molecular Formula:C₁₈H₂₅NO₄
Molecular Weight:319.401
Hs Code.:

Synonyms:[2-(3,4-Dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-8-ylidene)-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2-(3,4-Dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-8-ylidene)-amine

Chemical Property:

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Technology Process of [2-(3,4-Dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-8-ylidene)-amine

There total 1 articles about [2-(3,4-Dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-8-ylidene)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 129881-26-1
[2-(3,4-Dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-8-ylidene)-amine

Guidance literature:: In benzene; Heating; azeotropic removal of water;
DOI:10.3987/COM-88-4738

Reference yield:

: 79-04-9
chloroacetyl chloride

: 129881-26-1
[2-(3,4-Dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-8-ylidene)-amine

: 420086-58-4
2-chloro-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-N-(1,4-dioxa-spiro[4.5]dec-7-en-8-yl)-acetamide

Guidance literature:: With triethylamine; In toluene; at 20 ℃; for 3h;
DOI:10.1021/ol025534e

Reference yield:

: 129881-26-1
[2-(3,4-Dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-8-ylidene)-amine

: 420086-59-5
dithiocarbonic acid S-{[[2-(3,4-dimethoxy-phenyl)-ethyl]-(1,4-dioxa-spiro[4.5]dec-7-en-8-yl)-carbamoyl]-methyl} ester O-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / toluene / 3 h / 20 °C

2: 95 percent / acetonitrile / 2 h / 20 °C

With triethylamine; In toluene; acetonitrile;
DOI:10.1021/ol025534e