tert-butyl 4-amino-3-[[N-(tert-butoxycarbonyl)-N-phenethylamino]methyl]benzoate

Base Information

Chemical Name:tert-butyl 4-amino-3-[[N-(tert-butoxycarbonyl)-N-phenethylamino]methyl]benzoate
CAS No.:147290-70-8
Molecular Formula:C₂₅H₃₄N₂O₄
Molecular Weight:426.556
Hs Code.:

Synonyms:tert-butyl 4-amino-3-[[N-(tert-butoxycarbonyl)-N-phenethylamino]methyl]benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 4-amino-3-[[N-(tert-butoxycarbonyl)-N-phenethylamino]methyl]benzoate

Chemical Property:

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Technology Process of tert-butyl 4-amino-3-[[N-(tert-butoxycarbonyl)-N-phenethylamino]methyl]benzoate

There total 8 articles about tert-butyl 4-amino-3-[[N-(tert-butoxycarbonyl)-N-phenethylamino]methyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 147290-69-5
t-butyl 4-nitro-3-[N-(t-butyloxycarbonyl)-N-(2-phenyl-ethyl)aminomethyl]benzoate

: 147290-70-8
tert-butyl 4-amino-3-[[N-(tert-butoxycarbonyl)-N-phenethylamino]methyl]benzoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jm00001a003

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 147290-70-8
tert-butyl 4-amino-3-[[N-(tert-butoxycarbonyl)-N-phenethylamino]methyl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂

2: 91 percent / H₂ / Pd/C / ethyl acetate

With hydrogen; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm00001a003

Reference yield:

: 3113-71-1
3-methyl-4-nitrobenzoic acid

: 147290-70-8
tert-butyl 4-amino-3-[[N-(tert-butoxycarbonyl)-N-phenethylamino]methyl]benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / PhSO₂Cl, pyridine

2: N-bromosuccinimide, (PhCO₂)2 / CCl₄ / Heating

3: NaHCO₃ / tetrahydrofuran

4: 100 percent / CH₂Cl₂

5: 91 percent / H₂ / Pd/C / ethyl acetate

With pyridine; N-Bromosuccinimide; hydrogen; sodium hydrogencarbonate; benzenesulfonyl chloride; dibenzoyl peroxide; palladium on activated charcoal; In tetrahydrofuran; tetrachloromethane; dichloromethane; ethyl acetate;
DOI:10.1021/jm00001a003