dichloro-phenyl-[2]thienyl-methane

Base Information

• Chemical Name: dichloro-phenyl-[2]thienyl-methane
• CAS No.: 102417-61-8
• Molecular Formula: C₁₁H₈Cl₂S
• Molecular Weight: 243.157
• Mol file: 102417-61-8.mol

Synonyms:dichloro-phenyl-[2]thienyl-methane

Chemical Property of dichloro-phenyl-[2]thienyl-methane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dichloro-phenyl-[2]thienyl-methane

There total 2 articles about dichloro-phenyl-[2]thienyl-methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Benzoylthiophene (135-00-2) → dichloro-phenyl-[2]thienyl-methane (102417-61-8)

Guidance literature:

With phosphorus pentachloride; at 60 - 80 ℃;

Reference yield:

benzoyl chloride (98-88-4) → dichloro-phenyl-[2]thienyl-methane (102417-61-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminium chloride

2: phosphorus pentachloride / 60 - 80 °C

With aluminium trichloride; phosphorus pentachloride;

Reference yield:

dichloro-phenyl-[2]thienyl-methane (102417-61-8) → phenyl-2-thienylmethylenemalonaldehyde (84457-10-3)

Guidance literature:

Multi-step reaction with 2 steps

1: AgClO₄, CaCO₃ / nitromethane

2: H₂O, HClO₄, NaCl

With perchloric acid; water; silver perchlorate; calcium carbonate; sodium chloride; In nitromethane;

DOI:10.1055/s-1982-29954

upstream raw materials:

2-Benzoylthiophene

benzoyl chloride

Downstream raw materials:

phenyl-2-thienylmethylenemalonaldehyde