(N-(5,8-Dimethyl-9H carbazol-1-yl)-N-methyl-4-methoxybenzenesulfonamide)

Base Information

Chemical Name:(N-(5,8-Dimethyl-9H carbazol-1-yl)-N-methyl-4-methoxybenzenesulfonamide)
CAS No.:1334246-12-6
Molecular Formula:C₂₂H₂₂N₂O₃S
Molecular Weight:394.494
Hs Code.:

Synonyms:(N-(5,8-Dimethyl-9H carbazol-1-yl)-N-methyl-4-methoxybenzenesulfonamide)

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Chemical Property of (N-(5,8-Dimethyl-9H carbazol-1-yl)-N-methyl-4-methoxybenzenesulfonamide)

Chemical Property:

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Technology Process of (N-(5,8-Dimethyl-9H carbazol-1-yl)-N-methyl-4-methoxybenzenesulfonamide)

There total 6 articles about (N-(5,8-Dimethyl-9H carbazol-1-yl)-N-methyl-4-methoxybenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.28%

: 1334245-97-4
N-(5,8-dimethyl-9H-carbazol-1-yl)-4-methoxybenzenesulfonamide

: 74-88-4
methyl iodide

: 1334246-12-6
(N-(5,8-Dimethyl-9H carbazol-1-yl)-N-methyl-4-methoxybenzenesulfonamide)

Guidance literature:: N-(5,8-dimethyl-9H-carbazol-1-yl)-4-methoxybenzenesulfonamide; With potassium hydroxide; In ethanol; at 70 ℃; for 0.25h;

methyl iodide; In ethanol; at 70 ℃; for 1h;

Reference yield:

: 6960-46-9
ethyl 7-nitroindole-2-carboxylate

: 1334246-12-6
(N-(5,8-Dimethyl-9H carbazol-1-yl)-N-methyl-4-methoxybenzenesulfonamide)

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide; water / ethanol / 40 °C

2.1: copper(II) oxide / quinoline / 2 h / 194 °C

3.1: ammonium chloride; iron / isopropyl alcohol; water / 2 h / 60 °C

3.2: 3 h / 20 °C

4.1: toluene-4-sulfonic acid / ethanol / 6 h / Reflux

5.1: potassium hydroxide / ethanol / 0.25 h / 70 °C

5.2: 1 h / 70 °C

With water; iron; ammonium chloride; toluene-4-sulfonic acid; potassium hydroxide; copper(II) oxide; In quinoline; ethanol; water; isopropyl alcohol;

Reference yield:

: 6960-45-8
7-nitro-1H-indole-2-carboxylic acid

: 1334246-12-6
(N-(5,8-Dimethyl-9H carbazol-1-yl)-N-methyl-4-methoxybenzenesulfonamide)

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(II) oxide / quinoline / 2 h / 194 °C

2.1: ammonium chloride; iron / isopropyl alcohol; water / 2 h / 60 °C

2.2: 3 h / 20 °C

3.1: toluene-4-sulfonic acid / ethanol / 6 h / Reflux

4.1: potassium hydroxide / ethanol / 0.25 h / 70 °C

4.2: 1 h / 70 °C

With iron; ammonium chloride; toluene-4-sulfonic acid; potassium hydroxide; copper(II) oxide; In quinoline; ethanol; water; isopropyl alcohol;