Technology Process of C21H19N5O2S
There total 7 articles about C21H19N5O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap;
In
pyridine; dichloromethane;
at 0 - 80 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 - 80 °C
2: toluene-4-sulfonic acid / toluene / 3 h / Reflux
3: sodium t-butanolate / tert-butyl alcohol / 2 h / 80 °C
4: ethanol / 1.5 h / 80 °C
5: hydrogen / palladium 10% on activated carbon / methanol / 18 h / 760.05 Torr
6: dmap / dichloromethane; pyridine / 0 - 80 °C
With
dmap; hydrogen; N-ethyl-N,N-diisopropylamine; sodium t-butanolate;
palladium 10% on activated carbon; toluene-4-sulfonic acid;
In
tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; toluene; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 - 80 °C
3: toluene-4-sulfonic acid / toluene / 3 h / Reflux
4: sodium t-butanolate / tert-butyl alcohol / 2 h / 80 °C
5: ethanol / 1.5 h / 80 °C
6: hydrogen / palladium 10% on activated carbon / methanol / 18 h / 760.05 Torr
7: dmap / dichloromethane; pyridine / 0 - 80 °C
With
dmap; hydrogen; N-ethyl-N,N-diisopropylamine; sodium t-butanolate;
palladium 10% on activated carbon; toluene-4-sulfonic acid;
In
tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; toluene; tert-butyl alcohol;