methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside

Base Information

Chemical Name:methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside
CAS No.:122901-36-4
Molecular Formula:C₄₇H₅₇NO₁₇
Molecular Weight:907.966
Hs Code.:

methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside

Synonyms:methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside

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Chemical Property of methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside

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Technology Process of methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside

There total 7 articles about methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 67-56-1
methanol

: 122924-18-9
4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-α-D-glucopyranosyl bromide

: 122901-36-4
methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside

Guidance literature:: With silver perchlorate; silver carbonate; In dichloromethane; toluene; at -30 ℃; for 5h;

Reference yield:

: 106989-01-9
1L-2-azido-1,4,5,6-tetra-O-benzyl-2-desoxy-4-C-(benzyloxymethyl)-muco-inosit

: 122901-36-4
methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / NaBH₄ / 4 percent NiCl₂ / ethanol

2: propan-1-ol / 30 h / 90 °C

3: pyridine

4: 89 percent / BF₃-diethyl ether / 4 h / Ambient temperature

5: 157 mg / HBr / CH₂Cl₂ / 1 h / Ambient temperature

6: 53 percent / Ag₂CO₃, AgClO₄ / CH₂Cl₂; toluene / 5 h / -30 °C

With pyridine; sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen bromide; silver perchlorate; silver carbonate; nickel dichloride; In propan-1-ol; ethanol; dichloromethane; toluene;

Reference yield:

: 33208-46-7
1,6:3,4-Dianhydro-2-O-benzyl-β-D-galactopyranose

: 122901-36-4
methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-3,6-di-O-acetyl-2-O-benzyl-4-desoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: propan-1-ol / 30 h / 90 °C

2: pyridine

3: 89 percent / BF₃-diethyl ether / 4 h / Ambient temperature

4: 157 mg / HBr / CH₂Cl₂ / 1 h / Ambient temperature

5: 53 percent / Ag₂CO₃, AgClO₄ / CH₂Cl₂; toluene / 5 h / -30 °C

With pyridine; boron trifluoride diethyl etherate; hydrogen bromide; silver perchlorate; silver carbonate; In propan-1-ol; dichloromethane; toluene;