ethyl 3-(3-cyano-3-((2-(cyclohex-1-en-1-yl)ethyl)-amino)-2-oxoindolin-1-yl)-2-diazo-3-oxopropanoate

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Chemical Name:ethyl 3-(3-cyano-3-((2-(cyclohex-1-en-1-yl)ethyl)-amino)-2-oxoindolin-1-yl)-2-diazo-3-oxopropanoate
CAS No.:1351517-68-4
Molecular Formula:C₂₂H₂₃N₅O₄
Molecular Weight:421.456
Hs Code.:

Synonyms:ethyl 3-(3-cyano-3-((2-(cyclohex-1-en-1-yl)ethyl)-amino)-2-oxoindolin-1-yl)-2-diazo-3-oxopropanoate

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Chemical Property of ethyl 3-(3-cyano-3-((2-(cyclohex-1-en-1-yl)ethyl)-amino)-2-oxoindolin-1-yl)-2-diazo-3-oxopropanoate

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Technology Process of ethyl 3-(3-cyano-3-((2-(cyclohex-1-en-1-yl)ethyl)-amino)-2-oxoindolin-1-yl)-2-diazo-3-oxopropanoate

There total 4 articles about ethyl 3-(3-cyano-3-((2-(cyclohex-1-en-1-yl)ethyl)-amino)-2-oxoindolin-1-yl)-2-diazo-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 57072-87-4
chlorocarbonyl-diazo-acetic acid ethyl ester

: 1351517-66-2
3-((2-(cyclohex-1-en-1-yl)ethyl)amino)-2-oxoindoline-3-carbonitrile

: 1351517-68-4
ethyl 3-(3-cyano-3-((2-(cyclohex-1-en-1-yl)ethyl)-amino)-2-oxoindolin-1-yl)-2-diazo-3-oxopropanoate

Guidance literature:: With dmap; In dichloromethane; at 23 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.118

Reference yield:

: 3399-73-3
2-(1-cyclohexenyl)ethylamine

: 1351517-68-4
ethyl 3-(3-cyano-3-((2-(cyclohex-1-en-1-yl)ethyl)-amino)-2-oxoindolin-1-yl)-2-diazo-3-oxopropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / ethanol / 4 h / 23 °C / Inert atmosphere

2: hydrogenchloride / methanol; water / 24 h / 23 °C

3: dmap / dichloromethane / 16 h / 23 °C / Inert atmosphere

With hydrogenchloride; dmap; acetic acid; In methanol; ethanol; dichloromethane; water; 2: Strecker reaction;
DOI:10.1016/j.tet.2011.09.118

Reference yield:

: 1351517-65-1,508231-65-0
(Z)-3-((2-(cyclohex-1-en-1-yl)ethyl)imino)indolin-2-one

: 1351517-68-4
ethyl 3-(3-cyano-3-((2-(cyclohex-1-en-1-yl)ethyl)-amino)-2-oxoindolin-1-yl)-2-diazo-3-oxopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol; water / 24 h / 23 °C

2: dmap / dichloromethane / 16 h / 23 °C / Inert atmosphere

With hydrogenchloride; dmap; In methanol; dichloromethane; water; 1: Strecker reaction;
DOI:10.1016/j.tet.2011.09.118