N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine N'-methoxy-N'-methylamide

Base Information

Chemical Name:N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine N'-methoxy-N'-methylamide
CAS No.:254730-67-1
Molecular Formula:C₂₀H₂₀N₂O₄
Molecular Weight:352.39
Hs Code.:

Synonyms:N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine N'-methoxy-N'-methylamide

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Chemical Property of N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine N'-methoxy-N'-methylamide

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Technology Process of N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine N'-methoxy-N'-methylamide

There total 3 articles about N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine N'-methoxy-N'-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 254730-61-5
N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine

: 254730-67-1
N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine N'-methoxy-N'-methylamide

Guidance literature:: With triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1016/S0040-4020(99)00802-9

Reference yield:

: 17831-88-8
4-chloro-2H-1-benzopyran-2-one

: 254730-67-1
N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine N'-methoxy-N'-methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Et₃N / ethanol / 16 h / Heating

2: 71 percent / Et₃N; 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 4 h / 0 - 20 °C

With triethylamine; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; 1: Substitution / 2: Acylation;
DOI:10.1016/S0040-4020(99)00802-9

Reference yield:

: potassium; benzylamino-acetate

: 254730-67-1
N-benzyl-N-(2-oxo-2H-1-benzopyran-4-yl)glycine N'-methoxy-N'-methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Et₃N / ethanol / 16 h / Heating

2: 71 percent / Et₃N; 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 4 h / 0 - 20 °C

With triethylamine; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; 1: Substitution / 2: Acylation;
DOI:10.1016/S0040-4020(99)00802-9