[(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid

Base Information

• Chemical Name: [(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid
• CAS No.: 146831-92-7
• Molecular Formula: C₂₇H₂₈O₈
• Molecular Weight: 480.515

Synonyms:[(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid

Chemical Property of [(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid

Chemical Property:

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Technology Process of [(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid

There total 1 articles about [(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromophenylacetic acid (4870-65-9,31302-84-8) + sym-(hydroxy)dibenzo-16-crown-5 (78328-78-6) → [(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.07,12]tetracosa-1(24),7(12),8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid (146831-92-7)

Guidance literature:

With sodium hydride; In tetrahydrofuran; Yield given;

DOI:10.1021/ac00058a009

Reference yield: 100.0%

methanol (67-56-1) + [(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.07,12]tetracosa-1(24),7(12),8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid (146831-92-7) → [(2,6,13,16,19-pentaoxa-tricyclo[18.4.0.07,12]tetracosa-1(24),7,9,11,20,22-hexaen-4-yloxy)]-phenyl-acetic acid methyl ester

Guidance literature:

With sulfuric acid; for 12h; Heating;

DOI:10.1002/jhet.5570410503

Reference yield: 77.0%

[(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.07,12]tetracosa-1(24),7(12),8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid (146831-92-7) → [(+/-)-sym-dibenzo-16-crown-5-oxy]phenylacetonitrile

Guidance literature:

[(2,6,13,16,19-Pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-yloxy)]-phenyl-acetic acid; With oxalyl dichloride; In benzene; at 21 ℃; for 6h;

With 2,4-dinitrobenzenesulfonamide; triethylamine; In tetrahydrofuran; for 24h; Heating;

DOI:10.1016/S0040-4020(98)00581-X

upstream raw materials:

2-bromophenylacetic acid

sym-(hydroxy)dibenzo-16-crown-5

Downstream raw materials:

N-Benzyloxy-2-(2,6,13,16,19-pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-yloxy)-2-phenyl-acetamide

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