N-[(4-nitrophenyl)thio]-2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline

Base Information

Chemical Name:N-[(4-nitrophenyl)thio]-2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline
CAS No.:353754-56-0
Molecular Formula:C₂₇H₂₀Cl₂N₂O₄S
Molecular Weight:539.439
Hs Code.:

Synonyms:N-[(4-nitrophenyl)thio]-2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(4-nitrophenyl)thio]-2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline

Chemical Property:

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Technology Process of N-[(4-nitrophenyl)thio]-2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline

There total 3 articles about N-[(4-nitrophenyl)thio]-2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 937-32-6
4-nitrobenzenesulfenyl chloride

: 353754-50-4
2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline

: 353754-56-0
N-[(4-nitrophenyl)thio]-2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline

Guidance literature:: With triethylamine; In diethyl ether; at 0 ℃; for 2h;
DOI:10.1039/b100276g

Reference yield:

: 353754-49-1
2-(ethoxycarbonyl)-4,6-dibromoaniline

: 353754-56-0
N-[(4-nitrophenyl)thio]-2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / (PPh₃)4Pd; K₂CO₃ / benzene; ethanol; H₂O / 15 h / Heating

2: 48 percent / Et₃N / diethyl ether / 2 h / 0 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; triethylamine; In diethyl ether; ethanol; water; benzene;
DOI:10.1039/b100276g

Reference yield:

: 87-25-2
2-ethoxycarbonylaniline

: 353754-56-0
N-[(4-nitrophenyl)thio]-2,4-bis(4-chlorophenyl)-6-ethoxycarbonylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / benzyltrimethylammonium tribromide / CH₂Cl₂; methanol / 1 h / 20 °C

2: 90 percent / (PPh₃)4Pd; K₂CO₃ / benzene; ethanol; H₂O / 15 h / Heating

3: 48 percent / Et₃N / diethyl ether / 2 h / 0 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; benzyltrimethylammonium tribromide; potassium carbonate; triethylamine; In methanol; diethyl ether; ethanol; dichloromethane; water; benzene;
DOI:10.1039/b100276g