C₂₉H₃₈O₇

Base Information

Chemical Name:C₂₉H₃₈O₇
CAS No.:1320210-82-9
Molecular Formula:C₂₉H₃₈O₇
Molecular Weight:498.617
Hs Code.:

C<sub>29</sub>H<sub>38</sub>O<sub>7</sub>

Synonyms:C₂₉H₃₈O₇

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Chemical Property of C₂₉H₃₈O₇

Chemical Property:

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Technology Process of C₂₉H₃₈O₇

There total 7 articles about C₂₉H₃₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1320210-73-8
C₂₄H₃₀O₆

: 3282-30-2
pivaloyl chloride

: 1320210-82-9
C₂₉H₃₈O₇

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: 131310-61-7
(2R,4aR,6S,7R,8aS)-6-Methyl-2-phenyl-6-vinyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 1320210-82-9
C₂₉H₃₈O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere

2.1: ozone / methanol; dichloromethane / -78 °C

2.2: -78 - 20 °C

3.1: benzene / 2 h / Inert atmosphere; Reflux

4.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

5.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

5.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

6.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

6.2: Saturated solution

7.1: pyridine / dichloromethane / 0 °C / Inert atmosphere

With pyridine; titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; sodium hydride; diisobutylaluminium hydride; ozone; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; benzene; 3.1: Wittig reaction / 5.1: Sharpless epoxidation / 5.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: C₂₃H₂₆O₄

: 1320210-82-9
C₂₉H₃₈O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: ozone / methanol; dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: benzene / 2 h / Inert atmosphere; Reflux

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

4.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

4.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

5.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

5.2: Saturated solution

6.1: pyridine / dichloromethane / 0 °C / Inert atmosphere

With pyridine; titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; diisobutylaluminium hydride; ozone; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; benzene; 2.1: Wittig reaction / 4.1: Sharpless epoxidation / 4.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071