C₁₆H₁₄O₄

Base Information

Chemical Name:C₁₆H₁₄O₄
CAS No.:1489232-84-9
Molecular Formula:C₁₆H₁₄O₄
Molecular Weight:270.285
Hs Code.:

C<sub>16</sub>H<sub>14</sub>O<sub>4</sub>

Synonyms:C₁₆H₁₄O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₄O₄

Chemical Property:

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Technology Process of C₁₆H₁₄O₄

There total 10 articles about C₁₆H₁₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 67-56-1
methanol

: 1489232-53-2
C₁₅H₁₂O₄

: 1489232-84-9
C₁₆H₁₄O₄

Guidance literature:: With acetyl chloride; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2013.07.028

Reference yield:

: 836-42-0
4-benzyloxybenzyl chloride

: 1489232-84-9
C₁₆H₁₄O₄

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 60 °C

2: potassium hydroxide; water / methanol; tetrahydrofuran / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C

4: 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0 - 20 °C

5: rhodium (II) octanoate dimer / dichloromethane / 0 - 20 °C

6: barium hydroxide octahydrate / methanol; tetrahydrofuran / 0 - 20 °C

7: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran / 20 °C

8: acetyl chloride / 0 - 20 °C

With dmap; 4-toluenesulfonyl azide; rhodium (II) octanoate dimer; barium hydroxide octahydrate; palladium 10% on activated carbon; water; hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetyl chloride; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tetlet.2013.07.028

Reference yield:

: 22446-37-3
methyl (2-hydroxyphenyl)acetate

: 1489232-84-9
C₁₆H₁₄O₄

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 60 °C

2: potassium hydroxide; water / methanol; tetrahydrofuran / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C

4: 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0 - 20 °C

5: rhodium (II) octanoate dimer / dichloromethane / 0 - 20 °C

6: barium hydroxide octahydrate / methanol; tetrahydrofuran / 0 - 20 °C

7: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran / 20 °C

8: acetyl chloride / 0 - 20 °C

With dmap; 4-toluenesulfonyl azide; rhodium (II) octanoate dimer; barium hydroxide octahydrate; palladium 10% on activated carbon; water; hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetyl chloride; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tetlet.2013.07.028