boc-protected-4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-N'-phenylbenzohydrazide

Base Information

Chemical Name:boc-protected-4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-N'-phenylbenzohydrazide
CAS No.:1059147-29-3
Molecular Formula:C₃₆H₃₈N₆O₃
Molecular Weight:602.736
Hs Code.:

Synonyms:boc-protected-4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-N'-phenylbenzohydrazide

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Chemical Property of boc-protected-4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-N'-phenylbenzohydrazide

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Technology Process of boc-protected-4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-N'-phenylbenzohydrazide

There total 3 articles about boc-protected-4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-N'-phenylbenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1059145-38-8
N'-phenyl-4-((5,6,7,8-tetrahydroquinolin-8-ylamino)methyl)benzohydrazide

: 163798-87-6
1-Boc-2-chloromethylbenzimidazole

: 1059147-29-3
boc-protected-4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-N'-phenylbenzohydrazide

Guidance literature:: With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 65 ℃; for 24h;

Reference yield:

: 298181-83-6
5,6,7,8-tetrahydroquinolin-8-yl amine

: 1059147-29-3
boc-protected-4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-N'-phenylbenzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,2-dichloro-ethane / 0.17 h / 20 °C

1.2: 16 h / 20 °C

2.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / 65 °C

With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 1059147-58-8
4-formyl-N'-phenylbenzohydrazide

: 1059147-29-3
boc-protected-4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-N'-phenylbenzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,2-dichloro-ethane / 0.17 h / 20 °C

1.2: 16 h / 20 °C

2.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / 65 °C

With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; acetonitrile;