8bH-2a,4a,6a,8a-Tetraaza-8bl5-phosphapentaleno[1,6-cd]pentalene,octahydro- (9CI)

Base Information

Chemical Name:8bH-2a,4a,6a,8a-Tetraaza-8bl5-phosphapentaleno[1,6-cd]pentalene,octahydro- (9CI)
CAS No.:64317-97-1
Molecular Formula:C8H17 N4 P
Molecular Weight:200.224
Hs Code.:

Synonyms:Cyclenphosphorane;NSC 629375

Suppliers and Price of 8bH-2a,4a,6a,8a-Tetraaza-8bl5-phosphapentaleno[1,6-cd]pentalene,octahydro- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8bH-2a,4a,6a,8a-Tetraaza-8bl5-phosphapentaleno[1,6-cd]pentalene,octahydro- (9CI)

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 8bH-2a,4a,6a,8a-Tetraaza-8bl5-phosphapentaleno[1,6-cd]pentalene,octahydro- (9CI)

There total 2 articles about 8bH-2a,4a,6a,8a-Tetraaza-8bl5-phosphapentaleno[1,6-cd]pentalene,octahydro- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 63366-54-1
bis[bis(dimethylamino)phosphinyl]methane

: 64317-97-1
Cyclenphosphorane

: 14937-39-4
methyl-bis(dimethylamino)phosphine

Guidance literature:: With dimethyl amine; 1,4,7,10-tetraazacyclododecan; In toluene; at 115 ℃; for 0.916667h;
DOI:10.1080/10426509708044207

Reference yield: 71.0%

: 294-90-6
1,4,7,10-tetraazacyclododecan

: 64317-97-1
Cyclenphosphorane

: 14937-39-4
methyl-bis(dimethylamino)phosphine

Guidance literature:: With bis[bis(dimethylamino)phosphinyl]methane; dimethyl amine; In toluene; at 115 ℃; for 0.916667h;
DOI:10.1080/10426509708044207

Reference yield: 96.0%

: 10199-34-5,14056-88-3,15604-36-1
cis-dichlorobis(triphenylphosphine)platinum(II)

: 64317-97-1
cyclenphosphorane

: 108148-25-0
cis-((H₂cyclen)P)PtCl₂PPh₃}Cl

: 108148-24-9
{(eta.2-cyclenphosphorane)PtClPPh₃}

: 603-35-0
triphenylphosphine

Guidance literature:: In tetrahydrofuran; under N2, mixt. of phosphorane and Pt complex in THF was stirred for 12h, pptn.; volatiles removed in vac., residue washed (10 times hexane, 10 times THF (to dissolve the η2-complex), residue (cis complex) and washing (η2.-complex) pumped dry separately, each heated to 90°C under vac., elem. anal.;