N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

Base Information

Chemical Name:N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)
CAS No.:1351948-64-5
Molecular Formula:C₅₄H₄₇N₃O₆
Molecular Weight:833.984
Hs Code.:

Synonyms:N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

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Chemical Property of N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

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Technology Process of N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

There total 5 articles about N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1351948-46-3
N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 1351948-64-5
N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

Guidance literature:: With magnesium sulfate; acetic acid; In ethanol; dichloromethane; at 20 ℃; for 14.5h; Reflux;
DOI:10.1002/chem.201103221

Reference yield:

: 165261-27-8
2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

: 1351948-64-5
N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2 h / 100 °C

1.2: 24 h / 140 °C

2.1: zinc diacetate; 1H-imidazole / 2.5 h / 130 °C

3.1: magnesium sulfate; acetic acid / dichloromethane; ethanol / 14.5 h / 20 °C / Reflux

With 1H-imidazole; zinc diacetate; magnesium sulfate; acetic acid; In ethanol; dichloromethane; 1.1: |Diels-Alder Cycloaddition / 1.2: |Diels-Alder Cycloaddition;
DOI:10.1002/chem.201103221

Reference yield:

: 1351948-42-9
N-(1-hexylheptyl)benzo[ghi]perylene-3,4,6,7-tetracarboxylic-3,4-dicarboximide-6,7-anhydride

: 1351948-64-5
N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

Guidance literature:: Multi-step reaction with 2 steps

1: zinc diacetate; 1H-imidazole / 2.5 h / 130 °C

2: magnesium sulfate; acetic acid / dichloromethane; ethanol / 14.5 h / 20 °C / Reflux

With 1H-imidazole; zinc diacetate; magnesium sulfate; acetic acid; In ethanol; dichloromethane;
DOI:10.1002/chem.201103221