N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

Base Information

• Chemical Name: N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)
• CAS No.: 1351948-46-3
• Molecular Formula: C₄₇H₄₂N₂O₅
• Molecular Weight: 714.861

Synonyms:N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

Chemical Property of N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

Chemical Property:

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Technology Process of N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

There total 4 articles about N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-(1-hexylheptyl)-N′-[4-(1,3-dioxolan-2-yl)benzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide) (1351948-44-1) → N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide) (1351948-46-3)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; for 96h; Reflux;

DOI:10.1002/chem.201103221

Reference yield: 82.0%

N-(1-hexylheptyl)benzo[ghi]perylene-3,4,6,7-tetracarboxylic-3,4-dicarboximide-6,7-anhydride (1351948-42-9) + 4-(1,3-dioxacyclopent-2-yl)benzylamine (104566-44-1) → N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide) (1351948-46-3)

Guidance literature:

N-(1-hexylheptyl)benzo[ghi]perylene-3,4,6,7-tetracarboxylic-3,4-dicarboximide-6,7-anhydride; 4-(1,3-dioxacyclopent-2-yl)benzylamine; With 1H-imidazole; zinc diacetate; at 130 ℃; for 2.5h;

With hydrogenchloride; acetic acid;

DOI:10.1002/chem.201103221

Reference yield: 81.0%

N-(1-hexylheptyl)-N′-(4-hydroxymethylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide) (1351948-75-8) → N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide) (1351948-46-3)

Guidance literature:

With hydrogen bromide; In water; dimethyl sulfoxide; at 110 ℃; for 24h;

DOI:10.1002/chem.201103221

upstream raw materials:

N-(1-hexylheptyl)benzo[ghi]perylene-3,4,6,7-tetracarboxylic-3,4-dicarboximide-6,7-anhydride

4-(1,3-dioxacyclopent-2-yl)benzylamine

2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

N-(1-hexylheptyl)-N′-[4-(1,3-dioxolan-2-yl)benzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

Downstream raw materials:

N-(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

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