2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

Base Information

Chemical Name:2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione
CAS No.:165261-27-8
Molecular Formula:C₃₅H₃₇NO₂
Molecular Weight:503.684
Hs Code.:

Synonyms:2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

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Chemical Property of 2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

There total 2 articles about 2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 22513-16-2
1-hexylheptylamine

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 198-55-0
PERYLENE

: 110590-84-6
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

: 165261-27-8
2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

Guidance literature:: With 1H-imidazole; zinc diacetate; water; at 190 ℃; for 24h;

Reference yield: 4.0%

: 502637-04-9
N-(1-Hexylheptyl)perylene-3,4-dicarboxylic anhydride 9,10-dicarboximide

: 198-55-0
PERYLENE

: 165261-27-8
2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

Guidance literature:: With potassium hydroxide; at 205 ℃; for 22h;

Reference yield:

: 165261-27-8
2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

: 1351948-46-3
N-(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-3,4,6,7-bis(dicarboximide)

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2 h / 100 °C

1.2: 24 h / 140 °C

2.1: zinc diacetate; 1H-imidazole / 2.5 h / 130 °C

With 1H-imidazole; zinc diacetate; 1.1: |Diels-Alder Cycloaddition / 1.2: |Diels-Alder Cycloaddition;
DOI:10.1002/chem.201103221