1-(4,6-dimethylpyrimidin-2-yl)-5-(2,2,2-trifluoro-N-acetamide)-3-phenylpyrazole

Base Information

Chemical Name:1-(4,6-dimethylpyrimidin-2-yl)-5-(2,2,2-trifluoro-N-acetamide)-3-phenylpyrazole
CAS No.:1455243-31-8
Molecular Formula:C₁₇H₁₄F₃N₅O
Molecular Weight:361.326
Hs Code.:

Synonyms:1-(4,6-dimethylpyrimidin-2-yl)-5-(2,2,2-trifluoro-N-acetamide)-3-phenylpyrazole

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Chemical Property of 1-(4,6-dimethylpyrimidin-2-yl)-5-(2,2,2-trifluoro-N-acetamide)-3-phenylpyrazole

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Technology Process of 1-(4,6-dimethylpyrimidin-2-yl)-5-(2,2,2-trifluoro-N-acetamide)-3-phenylpyrazole

There total 3 articles about 1-(4,6-dimethylpyrimidin-2-yl)-5-(2,2,2-trifluoro-N-acetamide)-3-phenylpyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 926245-73-0
1-(4,6-dimethylpyrimidin-2-yl)-5-amino-3-phenylpyrazole

: 407-25-0
trifluoroacetic anhydride

: 1455243-31-8
1-(4,6-dimethylpyrimidin-2-yl)-5-(2,2,2-trifluoro-N-acetamide)-3-phenylpyrazole

Guidance literature:: In trifluoroacetic acid; for 0.25h; Heating;
DOI:10.1007/s00044-013-0751-9

Reference yield:

: 23906-13-0
2-hydrazino-4,6-dimethylpyrimidine

: 1455243-31-8
1-(4,6-dimethylpyrimidin-2-yl)-5-(2,2,2-trifluoro-N-acetamide)-3-phenylpyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / neat (no solvent) / 1.5 h / 70 - 80 °C

2: trifluoroacetic acid / 0.25 h / Heating

With toluene-4-sulfonic acid; In trifluoroacetic acid;
DOI:10.1007/s00044-013-0751-9

Reference yield:

: 614-16-4
Benzoylacetonitrile

: 1455243-31-8
1-(4,6-dimethylpyrimidin-2-yl)-5-(2,2,2-trifluoro-N-acetamide)-3-phenylpyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / neat (no solvent) / 1.5 h / 70 - 80 °C

2: trifluoroacetic acid / 0.25 h / Heating

With toluene-4-sulfonic acid; In trifluoroacetic acid;
DOI:10.1007/s00044-013-0751-9