C₂₇H₂₂N₂O₂S₂

Base Information

Chemical Name:C₂₇H₂₂N₂O₂S₂
CAS No.:1261276-25-8
Molecular Formula:C₂₇H₂₂N₂O₂S₂
Molecular Weight:470.616
Hs Code.:

C<sub>27</sub>H<sub>22</sub>N<sub>2</sub>O<sub>2</sub>S<sub>2</sub>

Synonyms:C₂₇H₂₂N₂O₂S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₂N₂O₂S₂

Chemical Property:

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Technology Process of C₂₇H₂₂N₂O₂S₂

There total 8 articles about C₂₇H₂₂N₂O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 29886-62-2
4-thiophen-2-yl-benzoic acid

: 1261276-94-1
N-cyclopropyl-5,6-dihydro-4H-benzo[b]thieno[2,3-d]azepine-2-carboxamide

: 1261276-25-8
C₂₇H₂₂N₂O₂S₂

Guidance literature:: 4-thiophen-2-yl-benzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

N-cyclopropyl-5,6-dihydro-4H-benzo[b]thieno[2,3-d]azepine-2-carboxamide; With pyridine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 50998-74-8
methyl N-tosylanthranilate

: 1261276-25-8
C₂₇H₂₂N₂O₂S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / butanone, 1-

2.1: potassium tert-butylate / toluene

3.1: trichlorophosphate / 5 h / 20 °C / Reflux

3.2: Cooling with ice

4.1: ethanol; sodium / 0.5 h / Cooling with ice

4.2: 3.5 h / 0 °C / Reflux

5.1: hydrogen bromide; acetic acid / Reflux

5.2: 6 h / Reflux

6.1: pyridine; HATU / 16 h / 20 °C / Inert atmosphere

7.1: oxalyl dichloride / N,N-dimethyl-formamide / 0.08 h / 20 °C

7.2: 2 h / 20 °C

With pyridine; oxalyl dichloride; ethanol; potassium tert-butylate; hydrogen bromide; sodium; potassium carbonate; acetic acid; HATU; trichlorophosphate; N,N-dimethyl-formamide; In butanone, 1-; toluene;

Reference yield:

: 134-20-3
2-carbomethoxyaniline

: 1261276-25-8
C₂₇H₂₂N₂O₂S₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine / dichloromethane / 4 h

2.1: potassium carbonate / butanone, 1-

3.1: potassium tert-butylate / toluene

4.1: trichlorophosphate / 5 h / 20 °C / Reflux

4.2: Cooling with ice

5.1: ethanol; sodium / 0.5 h / Cooling with ice

5.2: 3.5 h / 0 °C / Reflux

6.1: hydrogen bromide; acetic acid / Reflux

6.2: 6 h / Reflux

7.1: pyridine; HATU / 16 h / 20 °C / Inert atmosphere

8.1: oxalyl dichloride / N,N-dimethyl-formamide / 0.08 h / 20 °C

8.2: 2 h / 20 °C

With pyridine; oxalyl dichloride; ethanol; potassium tert-butylate; hydrogen bromide; sodium; potassium carbonate; acetic acid; HATU; trichlorophosphate; N,N-dimethyl-formamide; In dichloromethane; butanone, 1-; toluene;