1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime

Base Information

Chemical Name:1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime
CAS No.:1370339-80-2
Molecular Formula:C₂₂H₂₂ClN₇O
Molecular Weight:435.916
Hs Code.:

Synonyms:1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime

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Chemical Property of 1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime

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Technology Process of 1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime

There total 2 articles about 1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 133910-00-6
2-n-Butyl-4-chloro-1-[(2'-(2-triphenylmethyl-2H-tetrazol-5-yl)-1,1'-biphenyl-4-yl)methyl]-1H-imidazole-5-carboxaldehyde

: 1370339-80-2
1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime

Guidance literature:: With hydroxylamine hydrochloride; In ethanol; for 3h; Reflux;
DOI:10.1016/j.ejmech.2012.01.043

Reference yield:

: 124750-99-8
cozaar

: 1370339-80-2
1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonic acid; manganese(IV) oxide / tert-butyl alcohol / 16 h / Reflux

2: hydroxylamine hydrochloride; potassium hydrogencarbonate / ethanol; water / 16 h / 60 °C

With manganese(IV) oxide; methanesulfonic acid; hydroxylamine hydrochloride; potassium hydrogencarbonate; In ethanol; water; tert-butyl alcohol;

Reference yield: 48.0%

: 1370339-80-2
1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime

: 76-83-5
trityl chloride

: 1370339-81-3
2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetonitrile; for 3h; Reflux;
DOI:10.1016/j.ejmech.2012.01.043