2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime

Base Information

Chemical Name:2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime
CAS No.:1370339-81-3
Molecular Formula:C₆₀H₅₀ClN₇O
Molecular Weight:920.556
Hs Code.:

Synonyms:2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime

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Chemical Property of 2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime

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Technology Process of 2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime

There total 1 articles about 2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1370339-80-2
1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde oxime

: 76-83-5
trityl chloride

: 1370339-81-3
2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetonitrile; for 3h; Reflux;
DOI:10.1016/j.ejmech.2012.01.043

Reference yield: 43.0%

: 1370339-81-3
2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime

: 1370339-82-4
(2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazol-4-yl)methylamine

Guidance literature:: 2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 3.5h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.01.043

Reference yield:

: 1370339-81-3
2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carbaldehyde o-trityloxime

: 1370339-83-5
3-(3,4-bis-benzyloxy-phenyl)-N-(2-n-butyl-5-chloro-3-[2'-(2-trityl-2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazol-4-ylmethyl)propionamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / 0 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 20 h / 60 °C / Inert atmosphere

2.2: 4 h / 60 °C / Inert atmosphere

With lithium aluminium tetrahydride; 1,1'-carbonyldiimidazole; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2012.01.043