N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester

Base Information

Chemical Name:N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester
CAS No.:139225-06-2
Molecular Formula:C₁₇H₁₉NO₃
Molecular Weight:285.343
Hs Code.:

Synonyms:N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester

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Chemical Property of N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester

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Technology Process of N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester

There total 4 articles about N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67-56-1
methanol

: 139224-87-6
N-<(R)-2-hydroxy-1-phenylethyl>-(S)-α-aminobenzeneacetonitrile

: 139225-06-2
N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester

Guidance literature:: With hydrogenchloride; In diethyl ether; for 5h; Ambient temperature;
DOI:10.1016/0040-4020(95)00523-B

Reference yield:

: 139224-87-6
N-<(R)-2-hydroxy-1-phenylethyl>-(S)-α-aminobenzeneacetonitrile

: 139225-06-2
N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester

Guidance literature:: With hydrogenchloride; In methanol; for 5h; Ambient temperature;
DOI:10.1016/0040-4039(91)80544-G

Reference yield:

: 56613-80-0
D-2-phenylglycinol

: 139225-06-2
N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: CHCl₃ / 1 h / Ambient temperature; other aldehydes

2: methanol / 8 h / Ambient temperature

3: HCl / methanol / 5 h / Ambient temperature

With hydrogenchloride; In methanol; chloroform;
DOI:10.1016/0040-4039(91)80544-G