methyl N-[(Z)-4-{2-fluoro-4,4-dimethylpent-2-enyloxy}-2,5-dimethylphenyl]formimidate

Base Information

Chemical Name:methyl N-[(Z)-4-{2-fluoro-4,4-dimethylpent-2-enyloxy}-2,5-dimethylphenyl]formimidate
CAS No.:1384267-60-0
Molecular Formula:C₁₇H₂₄FNO₂
Molecular Weight:293.381
Hs Code.:

Synonyms:methyl N-[(Z)-4-{2-fluoro-4,4-dimethylpent-2-enyloxy}-2,5-dimethylphenyl]formimidate

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Chemical Property of methyl N-[(Z)-4-{2-fluoro-4,4-dimethylpent-2-enyloxy}-2,5-dimethylphenyl]formimidate

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Technology Process of methyl N-[(Z)-4-{2-fluoro-4,4-dimethylpent-2-enyloxy}-2,5-dimethylphenyl]formimidate

There total 6 articles about methyl N-[(Z)-4-{2-fluoro-4,4-dimethylpent-2-enyloxy}-2,5-dimethylphenyl]formimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1384267-70-2
(Z)-2-fluoro-4,4-dimethyl-1-(4-amino-2,5-dimethylphenoxy)penta-2-ene

: 149-73-5
trimethyl orthoformate

: 1384267-60-0
methyl N-[(Z)-4-{2-fluoro-4,4-dimethylpent-2-enyloxy}-2,5-dimethylphenyl]formimidate

Guidance literature:: With toluene-4-sulfonic acid; for 1h; Reflux;

Reference yield:

: 4775-69-3
1-bromo-4,4-dimethylpentan-2-one

: 1384267-60-0
methyl N-[(Z)-4-{2-fluoro-4,4-dimethylpent-2-enyloxy}-2,5-dimethylphenyl]formimidate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetonitrile / 1 h / Reflux

2: (bis-(2-methoxyethyl)amino)sulfur trufluoride / 5.5 h / 70 °C

3: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 3000.3 Torr

4: potassium tert-butylate / 1,4-dioxane / 7 h / Reflux

5: toluene-4-sulfonic acid / 1 h / Reflux

With potassium tert-butylate; hydrogen; potassium carbonate; toluene-4-sulfonic acid; (bis-(2-methoxyethyl)amino)sulfur trufluoride; palladium 10% on activated carbon; In 1,4-dioxane; ethanol; acetonitrile;

Reference yield:

: 3139-05-7
4-nitro-2,5-xylenol

: 1384267-60-0
methyl N-[(Z)-4-{2-fluoro-4,4-dimethylpent-2-enyloxy}-2,5-dimethylphenyl]formimidate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetonitrile / 1 h / Reflux

2: (bis-(2-methoxyethyl)amino)sulfur trufluoride / 5.5 h / 70 °C

3: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 3000.3 Torr

4: potassium tert-butylate / 1,4-dioxane / 7 h / Reflux

5: toluene-4-sulfonic acid / 1 h / Reflux

With potassium tert-butylate; hydrogen; potassium carbonate; toluene-4-sulfonic acid; (bis-(2-methoxyethyl)amino)sulfur trufluoride; palladium 10% on activated carbon; In 1,4-dioxane; ethanol; acetonitrile;