Aniline, 4,4'-thiobis(N,N-dimethyl-

Base Information

• Chemical Name: Aniline, 4,4'-thiobis(N,N-dimethyl-
• CAS No.: 13604-44-9
• Molecular Formula: C16H20N2S
• Molecular Weight: 272.414
• DSSTox Substance ID: DTXSID30159636
• Nikkaji Number: J3.479.840K
• Wikidata: Q83028001
• Mol file: 13604-44-9.mol

Synonyms:4,4'-Thiobis(N,N-dimethylaniline);Aniline, 4,4'-thiobis(N,N-dimethyl-;BRN 2811065;Benzenamine, 4,4'-thiobis(N,N-dimethyl-;13604-44-9;C16H20N2S;CBDivE_011413;SCHEMBL5701837;DTXSID30159636;C16-H20-N2-S;LS-19996

Chemical Property of Aniline, 4,4'-thiobis(N,N-dimethyl-

Chemical Property:

• XLogP3: 4.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 272.13471982
• Heavy Atom Count: 19
• Complexity: 226

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)SC2=CC=C(C=C2)N(C)C

Technology Process of Aniline, 4,4'-thiobis(N,N-dimethyl-

There total 23 articles about Aniline, 4,4'-thiobis(N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

N,N-dimethyl-aniline (121-69-7,77733-26-7) → bis(N,N-dimethylanilin-4-yl)sulfide (13604-44-9)

Guidance literature:

With morpholinesulfenyl chloride; boron trifluoride; In dichloromethane; at -78 - 25 ℃;

Reference yield:

chlorothio-trichloro-methane (594-42-3) + N,N-dimethyl-aniline (121-69-7,77733-26-7) → bis(N,N-dimethylanilin-4-yl)sulfide (13604-44-9) + crystal violet (548-62-9)

Guidance literature:

Reference yield:

4-(N,N-dimethylamino)phenyl disulfide (5397-29-5) + triphenylphosphine (603-35-0) → bis(N,N-dimethylanilin-4-yl)sulfide (13604-44-9) + triphenylphosphine sulfide (3878-45-3)

Guidance literature:

With benzene; beim Erhitzen des Reaktionsprodukts mit Wasser;

upstream raw materials:

5-amino-3H-1,2,4-dithiazole-3-thione

N,N-dimethyl-aniline

4-(N,N-dimethylamino)phenyl disulfide

bis-(4-dimethylamino-phenyl)-sulfoxide

Downstream raw materials:

N,N-dimethyl-4-tritylmercapto-aniline

N,N-dimethyl-aniline

bis-(4-dimethylamino-phenyl)-ether