6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol

Base Information

Chemical Name:6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol
CAS No.:889659-14-7
Molecular Formula:C₃₃H₄₁O₉P
Molecular Weight:612.657
Hs Code.:

Synonyms:6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol

Suppliers and Price of 6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol

There total 3 articles about 6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 124601-98-5
(-)-6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-myo-inositol

: 132741-50-5
2-(N,N-diisopropylamino)-5,6-benzo-1,3,2-dioxaphosphepane

: 889659-14-7
6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol

Guidance literature:: (-)-6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-myo-inositol; 2-(N,N-diisopropylamino)-5,6-benzo-1,3,2-dioxaphosphepane; With 1H-tetrazole; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

With tert.-butylhydroperoxide; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 889659-13-6
1-O-butyryl-2,3:4,5-di-O-cyclohexylidene-myo-inositol

: 889659-14-7
6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / methanol / 18 h / 20 °C

2.1: di(n-butyl)tin oxide / toluene / 3 h / Reflux

2.2: 12 h / -20 - 20 °C

3.1: 1H-tetrazole / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.2: 0 - 20 °C

With 1H-tetrazole; di(n-butyl)tin oxide; sodium hydroxide; In methanol; dichloromethane; toluene;

Reference yield:

: 100-39-0
benzyl bromide

: 889659-14-7
6-O-benzyl-2,3:4,5-di-O-cyclohexylidene-5-O-(o-xylylenedioxyphosphoryl)-D-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / toluene / 3 h / Reflux

1.2: 12 h / -20 - 20 °C

2.1: 1H-tetrazole / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.2: 0 - 20 °C

With 1H-tetrazole; di(n-butyl)tin oxide; In dichloromethane; toluene;