C₂₇H₃₁N₅O

Base Information

Chemical Name:C₂₇H₃₁N₅O
CAS No.:1201645-77-3
Molecular Formula:C₂₇H₃₁N₅O
Molecular Weight:441.576
Hs Code.:

C<sub>27</sub>H<sub>31</sub>N<sub>5</sub>O

Synonyms:C₂₇H₃₁N₅O

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Chemical Property of C₂₇H₃₁N₅O

Chemical Property:

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Technology Process of C₂₇H₃₁N₅O

There total 12 articles about C₂₇H₃₁N₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1201645-63-7
2-methyl-2-(4-((6-(4-methylpiperazin-1-yl)-3-aminoquinolin-4-yl)methyl)phenyl)propanenitrile

: 108-24-7
acetic anhydride

: 1201645-77-3
C₂₇H₃₁N₅O

Guidance literature:: With potassium acetate; In toluene;

Reference yield:

: 10075-50-0
5-bromo-1H-indole

: 1201645-77-3
C₂₇H₃₁N₅O

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / dimethyl sulfoxide / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: aluminum (III) chloride / dichloromethane / 0.17 h / 25 °C

2.2: 25 °C

3.1: sodium tetrahydroborate; trifluoroacetic acid / dichloromethane / 0 - 25 °C / Inert atmosphere

4.1: caesium carbonate / tetrahydrofuran; methanol / 2 h / 70 °C

5.1: ozone / N,N-dimethyl-formamide / 0.13 h / -5 °C

6.1: hydrogenchloride / acetone / 24 h

7.1: hydrogenchloride / water / 24 h

8.1: potassium acetate / ethanol / 5 h / Reflux

9.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 15 h / 14 °C

10.1: hydrogen / nickel / tetrahydrofuran / 25 °C / 760.05 Torr

11.1: potassium acetate / toluene

With hydrogenchloride; aluminum (III) chloride; sodium tetrahydroborate; hydrogen; potassium acetate; sodium hydride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; ozone; trifluoroacetic acid; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; nickel; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 40119-34-4
2-methyl-2-(4-methylphenyl)propionitrile

: 1201645-77-3
C₂₇H₃₁N₅O

Guidance literature:: Multi-step reaction with 12 steps

1.1: pyridine; potassium permanganate / water / 1 h / Reflux

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

3.1: aluminum (III) chloride / dichloromethane / 0.17 h / 25 °C

3.2: 25 °C

4.1: sodium tetrahydroborate; trifluoroacetic acid / dichloromethane / 0 - 25 °C / Inert atmosphere

5.1: caesium carbonate / tetrahydrofuran; methanol / 2 h / 70 °C

6.1: ozone / N,N-dimethyl-formamide / 0.13 h / -5 °C

7.1: hydrogenchloride / acetone / 24 h

8.1: hydrogenchloride / water / 24 h

9.1: potassium acetate / ethanol / 5 h / Reflux

10.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 15 h / 14 °C

11.1: hydrogen / nickel / tetrahydrofuran / 25 °C / 760.05 Torr

12.1: potassium acetate / toluene

With pyridine; hydrogenchloride; aluminum (III) chloride; sodium tetrahydroborate; potassium permanganate; oxalyl dichloride; hydrogen; potassium acetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; ozone; N,N-dimethyl-formamide; trifluoroacetic acid; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; nickel; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;