C₁₇H₁₄ClFN₂O₂

Base Information

Chemical Name:C₁₇H₁₄ClFN₂O₂
CAS No.:1398523-33-5
Molecular Formula:C₁₇H₁₄ClFN₂O₂
Molecular Weight:332.762
Hs Code.:

C<sub>17</sub>H<sub>14</sub>ClFN<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₇H₁₄ClFN₂O₂

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Chemical Property of C₁₇H₁₄ClFN₂O₂

Chemical Property:

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Technology Process of C₁₇H₁₄ClFN₂O₂

There total 4 articles about C₁₇H₁₄ClFN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1049117-55-6
C₁₅H₁₂ClFN₂O

: 64-19-7,77671-22-8
acetic acid

: 1398523-33-5
C₁₇H₁₄ClFN₂O₂

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 8h; Reflux;
DOI:10.1016/j.bmc.2012.08.020

Reference yield:

: 635-93-8
5-chlorosalicyclaldehyde

: 1398523-33-5
C₁₇H₁₄ClFN₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol; water / 0 - 20 °C

2: hydrazine hydrate / 8 h / 80 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 8 h / Reflux

With benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmc.2012.08.020

Reference yield:

: 403-42-9
1-(4-fluorophenyl)ethanone

: 1398523-33-5
C₁₇H₁₄ClFN₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol; water / 0 - 20 °C

2: hydrazine hydrate / 8 h / 80 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 8 h / Reflux

With benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmc.2012.08.020