[(2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-OH)Ru(PPh3)][B(C6H3(CF3)2-3,5)4]

Base Information

Chemical Name:[(2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-OH)Ru(PPh3)][B(C6H3(CF3)2-3,5)4]
CAS No.:912672-52-7
Molecular Formula:C₃₂H₁₂BF₂₄*C₅₂H₅₄GeOPRuS
Molecular Weight:1794.92
Hs Code.:

Synonyms:[(2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-OH)Ru(PPh3)][B(C6H3(CF3)2-3,5)4]

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Chemical Property of [(2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-OH)Ru(PPh3)][B(C6H3(CF3)2-3,5)4]

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Technology Process of [(2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-OH)Ru(PPh3)][B(C6H3(CF3)2-3,5)4]

There total 2 articles about [(2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-OH)Ru(PPh3)][B(C6H3(CF3)2-3,5)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: Brookhart's acid

: (2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-O)Ru(PPh3)

: 912672-52-7
[(2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-OH)Ru(PPh3)][B(C6H3(CF3)2-3,5)4]

Guidance literature:: In not given;
DOI:10.1021/ja711325f

Reference yield:

: 912672-45-8
[(2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-SH)Ru(PPh3)][B(C6H3(CF3)2-3,5)4]

: 7732-18-5
water

: 912672-52-7
[(2,6-dimesitylphenyl)(2,6-diethylphenyl)Ge(μ-S)(μ-OH)Ru(PPh3)][B(C6H3(CF3)2-3,5)4]

Guidance literature:: In tetrahydrofuran-d8; byproducts: H2S; Ge/Ru complex treated with 20 equiv. of H2O in THF-d10 at 293 K; not isolated, detcd. by NMR;
DOI:10.1039/c0cc03391j