6-(2,6-diisopropylanilino)fulvene

Base Information

Chemical Name:6-(2,6-diisopropylanilino)fulvene
CAS No.:734526-34-2
Molecular Formula:C₁₈H₂₃N
Molecular Weight:253.387
Hs Code.:

Synonyms:6-(2,6-diisopropylanilino)fulvene

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Chemical Property of 6-(2,6-diisopropylanilino)fulvene

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Technology Process of 6-(2,6-diisopropylanilino)fulvene

There total 1 articles about 6-(2,6-diisopropylanilino)fulvene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 696-68-4
6-(dimethylamino)fulvene

: lithium (2,6-diisopropylphenyl)amide

: 734526-34-2
6-(2,6-diisopropylanilino)fulvene

: 24544-04-5
2,6-diisopropylbenzenamine

Guidance literature:: 6-(dimethylamino)fulvene; lithium (2,6-diisopropylphenyl)amide; In diethyl ether; Inert atmosphere;

With acetylacetone; In diethyl ether; at -40 ℃; Inert atmosphere;

Reference yield: 87.0%

: 734526-34-2
6-(2,6-diisopropylanilino)fulvene

: 10026-11-6
zirconium(IV) chloride

: 6921-34-2
benzylmagnesium chloride

: 1186435-09-5
(C₅H₄CHN-2,6-diisopropylphenyl)2Zr(benzyl)2

Guidance literature:: In diethyl ether; under Ar, protected from direct light; Et2O added to ZrCl4 at -78°C; stirred at -78°C; soln. of PhCH2MgCl in Et2O added at -78°C; stirred (room temp., 1 h); Et2O soln. of ligand added at -78°C; stirred (room temp., 1 h); kept at -20°C overnight; volatiles removed under vac.; extd. (pentane); filtered; solvent evapd. in vac.; washed (pentane); dried under vac.; additional amt. of ppt. obtained from pentane washings at room temp. for several d; elem. anal.;
DOI:10.1021/om9004093