2-(3-Phenylpropylidene)cyclopentan-1-one

Base Information

Chemical Name:2-(3-Phenylpropylidene)cyclopentan-1-one
CAS No.:54322-81-5
Molecular Formula:C14H16 O
Molecular Weight:200.28
Hs Code.:
European Community (EC) Number:259-099-6
DSSTox Substance ID:DTXSID5068946
Nikkaji Number:J266.863G
Mol file:54322-81-5.mol

Synonyms:2-(3-Phenylpropylidene)cyclopentan-1-one;DTXSID5068946

Suppliers and Price of 2-(3-Phenylpropylidene)cyclopentan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-(3-Phenylpropylidene)cyclopentan-1-one

Chemical Property:

Vapor Pressure:0.000128mmHg at 25°C
Boiling Point:334.4°C at 760 mmHg
Flash Point:141.7°C
PSA：17.07000
Density:1.114g/cm³
LogP:3.29860
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:200.120115130
Heavy Atom Count:15
Complexity:246

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=CCCC2=CC=CC=C2)C(=O)C1
Isomeric SMILES:C1C/C(=C\CCC2=CC=CC=C2)/C(=O)C1

Technology Process of 2-(3-Phenylpropylidene)cyclopentan-1-one

There total 4 articles about 2-(3-Phenylpropylidene)cyclopentan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 201230-82-2
carbon monoxide

: 120-92-3
cyclopentanone

: 54322-81-5
2-(3-phenylpropylidene)-cyclopentanone

: 2-(2-phenylpropylidene)-cyclopentanone

Guidance literature:: With bis(benzonitrile)dichloroplatinum(II); hydrogen; toluene-4-sulfonic acid; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; tin(ll) chloride; at 100 ℃; for 24h; under 60006 Torr; Overall yield = 41 %; Schlenk technique;
DOI:10.1016/j.jorganchem.2018.04.031

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 19980-43-9
1-(trimethylsilyloxy)cyclopentene

: 54322-81-5
2-(3-phenylpropylidene)-cyclopentanone

Guidance literature:: With titanium tetrachloride; In dichloromethane;
DOI:10.1021/ja00831a019

Reference yield:

: 120-92-3
cyclopentanone

: 54322-81-5
2-(3-phenylpropylidene)-cyclopentanone

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 4 - 8 °C

2: Et₃N / CH₂Cl₂

With triethylamine; In dichloromethane;