4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-arabinitol

Base Information

Chemical Name:4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-arabinitol
CAS No.:154802-24-1
Molecular Formula:C₁₄H₁₇F₃O₄
Molecular Weight:306.282
Hs Code.:

Synonyms:4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-arabinitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-arabinitol

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Technology Process of 4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-arabinitol

There total 2 articles about 4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-arabinitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 3-O-benzyl-2,4-O-ethylidene-D-erythrose

: 154673-21-9
4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-ribitol

: 154802-24-1
4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-arabinitol

Guidance literature:: With hydrogenchloride; tetraethylammonium fluoride; Yield given. Multistep reaction; 1.) THF, -10 deg C, 5 min, 2.) EtOH, RT, 5 min;
DOI:10.1016/S0040-4039(00)61400-4

Reference yield:

: 4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoro-D-erythro-2-pentulose

: 154673-21-9
4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-ribitol

: 154802-24-1
4-O-benzyl-1-desoxy-3,5-O-ethylidene-1,1,1-trifluoromethyl-D-arabinitol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; at -78 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1016/0040-4020(94)00993-5