ethyl 2-(diethylamino)-4-oxo-3,5-diphenyl-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidine-7-carboxylate

Base Information

Chemical Name:ethyl 2-(diethylamino)-4-oxo-3,5-diphenyl-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidine-7-carboxylate
CAS No.:1375969-42-8
Molecular Formula:C₂₅H₂₆N₄O₃
Molecular Weight:430.506
Hs Code.:

Synonyms:ethyl 2-(diethylamino)-4-oxo-3,5-diphenyl-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidine-7-carboxylate

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Chemical Property of ethyl 2-(diethylamino)-4-oxo-3,5-diphenyl-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidine-7-carboxylate

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Technology Process of ethyl 2-(diethylamino)-4-oxo-3,5-diphenyl-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidine-7-carboxylate

There total 8 articles about ethyl 2-(diethylamino)-4-oxo-3,5-diphenyl-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidine-7-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₂N₄O₄

: 1375969-42-8
ethyl 2-(diethylamino)-4-oxo-3,5-diphenyl-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidine-7-carboxylate

Guidance literature:: With sodium ethanolate; In ethanol; at 20 ℃; for 2h; regioselective reaction;
DOI:10.5012/bkcs.2014.35.2.617

Reference yield:

: C₂₃H₂₁N₃O₄

: 1375969-42-8
ethyl 2-(diethylamino)-4-oxo-3,5-diphenyl-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidine-7-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 5 h

2: sodium ethanolate / ethanol / 2 h / 20 °C

With sodium ethanolate; In ethanol; dichloromethane;
DOI:10.5012/bkcs.2014.35.2.617

Reference yield:

: 2305-54-6
2-(Anilinomethylen)-2-cyanessigsaeure-ethylester

: 1375969-42-8
ethyl 2-(diethylamino)-4-oxo-3,5-diphenyl-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidine-7-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate

2: sodium ethanolate

3: hexachloroethane; triethylamine / acetonitrile / 6 h / 20 °C

4: dichloromethane / 1 h / 20 °C / Inert atmosphere

5: dichloromethane / 5 h

6: sodium ethanolate / ethanol / 2 h / 20 °C

With hexachloroethane; sodium ethanolate; potassium carbonate; triethylamine; In ethanol; dichloromethane; acetonitrile;
DOI:10.5012/bkcs.2014.35.2.617