diethyl 1-phenyl-3-((triphenylphosphoranylidene)amino)-1H-pyrrole-2,4-dicarboxylate

Base Information

Chemical Name:diethyl 1-phenyl-3-((triphenylphosphoranylidene)amino)-1H-pyrrole-2,4-dicarboxylate
CAS No.:1427690-28-5
Molecular Formula:C₃₄H₃₁N₂O₄P
Molecular Weight:562.605
Hs Code.:

Synonyms:diethyl 1-phenyl-3-((triphenylphosphoranylidene)amino)-1H-pyrrole-2,4-dicarboxylate

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Chemical Property of diethyl 1-phenyl-3-((triphenylphosphoranylidene)amino)-1H-pyrrole-2,4-dicarboxylate

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Technology Process of diethyl 1-phenyl-3-((triphenylphosphoranylidene)amino)-1H-pyrrole-2,4-dicarboxylate

There total 5 articles about diethyl 1-phenyl-3-((triphenylphosphoranylidene)amino)-1H-pyrrole-2,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 59021-45-3
3-amino-1-phenyl-pyrrol-2,4-dicarbonsaeurediethylester

: 603-35-0
triphenylphosphine

: 1427690-28-5
diethyl 1-phenyl-3-((triphenylphosphoranylidene)amino)-1H-pyrrole-2,4-dicarboxylate

Guidance literature:: With hexachloroethane; triethylamine; In acetonitrile; at 20 ℃; for 6h;
DOI:10.5012/bkcs.2014.35.2.617

Reference yield:

: 2305-54-6
2-(Anilinomethylen)-2-cyanessigsaeure-ethylester

: 1427690-28-5
diethyl 1-phenyl-3-((triphenylphosphoranylidene)amino)-1H-pyrrole-2,4-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate

2: sodium ethanolate

3: hexachloroethane; triethylamine / acetonitrile / 6 h / 20 °C

With hexachloroethane; sodium ethanolate; potassium carbonate; triethylamine; In acetonitrile;
DOI:10.5012/bkcs.2014.35.2.617

Reference yield:

: 59021-46-4
C₁₆H₁₈N₂O₄

: 1427690-28-5
diethyl 1-phenyl-3-((triphenylphosphoranylidene)amino)-1H-pyrrole-2,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium ethanolate

2: hexachloroethane; triethylamine / acetonitrile / 6 h / 20 °C

With hexachloroethane; sodium ethanolate; triethylamine; In acetonitrile;
DOI:10.5012/bkcs.2014.35.2.617