bis<(8-tert-butyldiphenylsilyloxy-2-quinolyl)methyl> methylphosphopnate

Base Information

Chemical Name:bis<(8-tert-butyldiphenylsilyloxy-2-quinolyl)methyl> methylphosphopnate
CAS No.:168204-26-0
Molecular Formula:C₅₃H₅₅N₂O₅PSi₂
Molecular Weight:887.175
Hs Code.:

Synonyms:bis<(8-tert-butyldiphenylsilyloxy-2-quinolyl)methyl> methylphosphopnate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis<(8-tert-butyldiphenylsilyloxy-2-quinolyl)methyl> methylphosphopnate

Chemical Property:

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Technology Process of bis<(8-tert-butyldiphenylsilyloxy-2-quinolyl)methyl> methylphosphopnate

There total 5 articles about bis<(8-tert-butyldiphenylsilyloxy-2-quinolyl)methyl> methylphosphopnate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 676-97-1
methylphosphonic acid dichloroanhydride

: 155933-77-0
<8-<(tert-butyldiphenylsilyl)oxy>quinolyl>methanol

: 168204-26-0
bis<(8-tert-butyldiphenylsilyloxy-2-quinolyl)methyl> methylphosphopnate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/ja00133a013

Reference yield:

: 826-81-3
2-methyl-8-quinolinol

: 168204-26-0
bis<(8-tert-butyldiphenylsilyloxy-2-quinolyl)methyl> methylphosphopnate

Guidance literature:: Multi-step reaction with 4 steps

1: 84.1 percent / imidazole / dimethylformamide / 72 h / Ambient temperature

2: 76.7 percent / SeO₂ / dioxane / 24 h / 75 °C

3: 93.8 percent / NaBH₄ / ethanol / 6 h / Ambient temperature

4: 76 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

With 1H-imidazole; sodium tetrahydroborate; selenium(IV) oxide; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00133a013

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 168204-26-0
bis<(8-tert-butyldiphenylsilyloxy-2-quinolyl)methyl> methylphosphopnate

Guidance literature:: Multi-step reaction with 4 steps

1: 84.1 percent / imidazole / dimethylformamide / 72 h / Ambient temperature

2: 76.7 percent / SeO₂ / dioxane / 24 h / 75 °C

3: 93.8 percent / NaBH₄ / ethanol / 6 h / Ambient temperature

4: 76 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

With 1H-imidazole; sodium tetrahydroborate; selenium(IV) oxide; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00133a013