N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine

Base Information

Chemical Name:N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine
CAS No.:1447992-76-8
Molecular Formula:C₂₁H₂₉N₃O
Molecular Weight:339.481
Hs Code.:

N<sup>1</sup>-{2-(4-morpholinyl)phenyl}-N<sup>2</sup>-(2,4,6-trimethylphenyl)-1,2-ethanediamine

Synonyms:N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine

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Chemical Property of N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine

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Technology Process of N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine

There total 1 articles about N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 444325-38-6
N-2,4,6-trimethylphenyl-(1,2-diaminoethane)

: 87698-82-6
4-(2-bromophenyl)morpholine

: 1447992-76-8
N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine

Guidance literature:: With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; sodium t-butanolate; In toluene; at 110 ℃; for 2.5h; regioselective reaction; Inert atmosphere; Glovebox;
DOI:10.1139/cjc-2013-0132

Reference yield: 88.0%

: 13826-83-0
ammonium tetrafluroborate

: 1447992-76-8
N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine

: 122-51-0
orthoformic acid triethyl ester

: 1447992-82-6
[1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate

Guidance literature:: at 110 ℃; for 0.5h; Inert atmosphere;
DOI:10.1139/cjc-2013-0132

Reference yield: 69.0%

: 1447992-76-8
N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine

: 122-51-0
orthoformic acid triethyl ester

: 1447992-80-4
[1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] chloride

Guidance literature:: N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine; With hydrogenchloride; In 1,4-dioxane; diethyl ether; at 0 ℃; Inert atmosphere;

orthoformic acid triethyl ester; at 110 ℃; for 0.5h; Inert atmosphere;
DOI:10.1139/cjc-2013-0132