<(benzyloxy)methyl>(tert-butyl)methylsilane

Base Information

• Chemical Name: <(benzyloxy)methyl>(tert-butyl)methylsilane
• CAS No.: 138380-19-5
• Molecular Formula: C₁₃H₂₂OSi
• Molecular Weight: 222.403
• Mol file: 138380-19-5.mol

Synonyms:<(benzyloxy)methyl>(tert-butyl)methylsilane

Chemical Property of <(benzyloxy)methyl>(tert-butyl)methylsilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <(benzyloxy)methyl>(tert-butyl)methylsilane

There total 4 articles about <(benzyloxy)methyl>(tert-butyl)methylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzyloxy-benzyloxymethyl-tert-butyl-methyl-silane → <(benzyloxy)methyl>(tert-butyl)methylsilane (138380-19-5)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; pentane; for 4.5h; Yield given;

DOI:10.1002/hlca.19910740712

Reference yield:

(chloromethyl)bis(benzyloxy)methylsilane (138380-14-0) → <(benzyloxy)methyl>(tert-butyl)methylsilane (138380-19-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 1) NaH / 1) THF, 23 deg C, 3 h 2) 23 deg C, 6 h

2: diethyl ether; pentane / 0.5 h / 0 °C

3: LiAlH₄ / diethyl ether; pentane / 4.5 h

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether; pentane;

DOI:10.1002/hlca.19910740712

Reference yield:

bis(benzyloxy)<(benzyloxy)methyl>methylsilane (138380-16-2) → <(benzyloxy)methyl>(tert-butyl)methylsilane (138380-19-5)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; pentane / 0.5 h / 0 °C

2: LiAlH₄ / diethyl ether; pentane / 4.5 h

With lithium aluminium tetrahydride; In diethyl ether; pentane;

DOI:10.1002/hlca.19910740712

upstream raw materials:

(chloromethyl)bis(benzyloxy)methylsilane

bis(benzyloxy)<(benzyloxy)methyl>methylsilane

benzyl alcohol

Downstream raw materials:

1-(Benzyloxymethyl-tert-butyl-methyl-silanyl)-1-phenyl-ethanol

<(benzyloxy)methyl>(tert-butyl)(1-ethoxyethenyl)methylsilane

<<(benzyloxy)methyl>(tert-butyl)methylsilyl> methyl ketone

1-(Benzyloxymethyl-tert-butyl-methyl-silanyl)-ethanol