9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone

Base Information

• Chemical Name: 9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone
• CAS No.: 130296-39-8
• Molecular Formula: C₄₃H₄₇NO₅
• Molecular Weight: 657.85

Synonyms:9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone

Chemical Property of 9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone

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Technology Process of 9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone

There total 1 articles about 9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.1%

N,N’-bis-(10-nonadecyl)perylene-3,4,9,10-tetracarboxylic acid diimide (130296-48-9) → 9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone (130296-39-8) + perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8)

Guidance literature:

With potassium hydroxide; In tert-butyl alcohol; Heating;

Reference yield: 80.0%

9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone (130296-39-8) + 2-(3-aminopropyl)-N,N,N',N'-tetramethyl-1,4-benzenediamine (852695-06-8) → N-(9-nonadecyl)-N'-(3-[2-(N'',N'',N''',N'''-tetramethyl-1,4-benzenediaminyl)propyl])perylene-4,5,9,10-bis(dicarboximide)

Guidance literature:

In toluene; for 4h; Heating;

DOI:10.1021/jo035409w

Reference yield: 73.0%

4-vinyl benzylamine (1520-21-4,25086-42-4) + 9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone (130296-39-8) → N-vinyl-N'-(10-nonadecyl)perylene-3,4,9,10-tetracarboxylic diimide

Guidance literature:

With zinc diacetate; In quinoline; at 160 ℃; for 4h; Inert atmosphere;

DOI:10.1016/j.dyepig.2014.11.009

upstream raw materials:

N,N’-bis-(10-nonadecyl)perylene-3,4,9,10-tetracarboxylic acid diimide

Downstream raw materials:

N-(1-nonyldecyl)-N'-(4-iodophenyl)perylene diimide

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